Cromatogramma intero: estratto cdg con etanolo

2o picco (piccolo): limonene

3o picco (piccolo): methyl salicylate

4o picco: eugenol e isomeri

5o e 7o picco: alpha-cubebene

8o picco: phenol… (isomero dell’eugenolo)

9o picco (piccolo): naphtalene… (sporattutto)

6o picco: caryophyllene oxide (max 74%) e altri

TIC: CDGET.D chiodo di garofano estratto etanolo Peak# Ret Time Type Width Area Start Time End Time 1 0.228 PV 0.023 887629 0.204 0.256 2 0.405 PV 0.014 689444 0.392 0.442 3 0.556 VV 0.014 643159 0.542 0.573 4 0.623 VV 0.022 1087534 0.611 0.653 5 0.710 VV 0.028 1300843 0.688 0.757 6 0.778 VV 0.018 785565 0.757 0.799 7 1.051 VV 0.014 655396 1.039 1.067 8 1.317 VV 0.019 1067926 1.287 1.343 9 1.361 VV 0.017 788637 1.343 1.374 10 1.419 VV 0.017 610367 1.396 1.440 11 1.510 VV 0.011 542373 1.498 1.526 12 1.726 VV 0.020 708992 1.691 1.735 13 1.824 VV 0.016 6564515 1.778 1.847 14 1.859 VV 0.018 1298079 1.847 1.866 15 1.952 VV 0.050 78047856 1.866 1.965 16 1.976 VV 0.056 72792015 1.965 2.030 17 2.038 VV 0.109 99561795 2.030 2.159 18 2.184 VV 0.085 70946360 2.159 2.295 19 2.317 VV 0.039 24211689 2.295 2.373 20 2.681 VV 0.023 4022238 2.669 2.709 21 3.227 VV 0.024 2167268 3.210 3.270 22 3.621 VV 0.012 862398 3.604 3.634 23 3.646 VV 0.010 581743 3.634 3.658 24 3.816 BV 0.016 705423 3.783 3.839 25 3.858 PV 0.014 793446 3.839 3.896 26 3.913 PV 0.012 781630 3.896 3.931 27 4.029 VV 0.021 967018 3.981 4.055 28 4.288 VV 0.020 865393 4.278 4.310 29 4.319 VV 0.019 1081015 4.310 4.357 30 4.459 VV 0.020 906053 4.416 4.473 31 4.484 VV 0.013 651624 4.473 4.503 32 4.514 VV 0.015 688290 4.503 4.537 33 4.571 PV 0.013 743837 4.555 4.583 34 4.617 VV 0.014 563252 4.603 4.633 35 4.653 VV 0.026 1280488 4.633 4.718 36 4.728 VV 0.012 501295 4.718 4.744 37 4.805 VV 0.022 934258 4.782 4.834 38 4.874 VV 0.012 567753 4.863 4.889 39 4.914 VV 0.025 850117 4.889 4.927 40 4.945 VV 0.020 719185 4.927 4.982 41 4.994 VV 0.010 453122 4.982 5.006 42 5.142 VV 0.014 734687 5.128 5.160 43 5.170 VV 0.013 533227 5.160 5.190 44 5.201 VV 0.036 1890029 5.190 5.294 45 5.413 VV 0.016 577698 5.402 5.437 46 5.576 VV 0.011 395388 5.566 5.585 47 5.596 VV 0.015 733296 5.585 5.613 48 5.625 VV 0.013 765757 5.613 5.647 49 5.716 VV 0.015 835727 5.706 5.744 50 5.778 VV 0.029 1234757 5.761 5.808 51 5.821 VV 0.017 682246 5.808 5.841 52 5.924 VV 0.023 997207 5.897 5.945 53 6.019 VV 0.016 782777 5.995 6.033 54 6.110 VV 0.028 1073299 6.055 6.121 55 6.207 VV 0.016 744710 6.187 6.217 56 6.384 PV 0.022 922796 6.356 6.394 57 6.406 VV 0.013 689207 6.394 6.416 58 6.444 VV 0.021 1112553 6.433 6.472 59 6.484 VV 0.027 1552483 6.472 6.521 60 6.534 VV 0.024 1384491 6.521 6.568 61 6.581 VV 0.021 1274218 6.568 6.603 62 6.837 VV 0.067 22930765 6.723 6.940 63 6.984 VV 0.018 1290247 6.966 6.996 64 7.081 VV 0.031 1677043 7.070 7.127 65 7.257 VV 0.010 598766 7.248 7.268 66 7.337 VV 0.017 829861 7.327 7.362 67 7.415 VV 0.013 757921 7.400 7.425 68 7.439 VV 0.030 2382442 7.425 7.472 69 7.652 VV 0.017 881689 7.639 7.681 70 7.749 VV 0.027 1284508 7.722 7.770 71 7.796 VV 0.021 882971 7.770 7.807 72 7.835 VV 0.031 1456891 7.807 7.862 73 7.889 VV 0.027 2154219 7.862 7.907 74 7.917 VV 0.019 975628 7.907 7.930 75 8.035 VV 0.033 1707376 8.025 8.073 76 8.176 VV 0.023 1085922 8.164 8.200 77 8.424 VV 0.026 1166416 8.413 8.469 78 8.489 VV 0.017 766179 8.469 8.501 79 8.562 VV 0.023 1031115 8.541 8.600 80 8.692 VV 0.025 1619561 8.619 8.703 81 8.853 VV 0.012 526387 8.841 8.865 82 8.964 VV 0.032 1450073 8.913 8.984 83 9.140 VV 0.015 565539 9.124 9.150 84 9.423 VV 0.039 2528003 9.347 9.432 85 9.447 VV 0.042 2551449 9.432 9.486 86 9.637 VV 0.024 871318 9.621 9.669 87 9.691 VV 0.018 798785 9.669 9.703 88 9.742 VV 0.022 1091733 9.725 9.756 89 9.922 VV 0.024 1006259 9.895 9.951 90 9.963 VV 0.018 679155 9.951 9.994 91 10.028 VV 0.021 917012 9.994 10.041 92 10.288 VV 0.015 834438 10.277 10.301 93 10.311 VV 0.013 696684 10.301 10.324 94 10.408 VV 0.052 12048104 10.324 10.456 95 10.467 VV 0.020 1932497 10.456 10.484 96 10.619 VV 0.017 748074 10.605 10.630 97 11.464 VV 0.016 661042 11.439 11.473 98 11.514 VV 0.016 838111 11.502 11.534 99 11.601 PV 0.013 595405 11.590 11.617 100 11.631 VV 0.012 501949 11.617 11.640 101 11.676 VV 0.013 507220 11.666 11.686 102 11.807 VV 0.036 2002520 11.751 11.816 103 11.827 VV 0.017 1310149 11.816 11.837 104 11.849 VV 0.022 1446497 11.837 11.862 105 11.871 VV 0.034 2167792 11.862 11.914 106 11.969 VV 0.022 1264168 11.954 12.008 107 12.069 VV 0.016 688783 12.054 12.082 108 12.145 PV 0.019 914167 12.127 12.170 109 12.283 VV 0.017 592066 12.271 12.306 110 12.646 PV 0.017 611836 12.634 12.697 111 12.869 VV 0.020 880640 12.854 12.899 112 13.096 PV 0.013 485471 13.080 13.107 113 13.167 VV 0.016 616408 13.147 13.178 114 13.201 VV 0.022 927371 13.178 13.219 115 13.240 VV 0.020 804616 13.219 13.263 116 13.396 VV 0.021 898779 13.377 13.434 117 13.590 PV 0.016 543436 13.579 13.608 118 13.620 VV 0.037 1472168 13.608 13.682 119 13.857 VV 0.025 1020596 13.846 13.900 120 14.369 VV 0.021 764447 14.332 14.387 121 14.427 VV 0.022 966954 14.387 14.450 122 15.096 VV 0.251 1446822593 14.513 15.164 123 15.174 VV 0.021 1629296 15.164 15.191 124 15.239 VV 0.034 2187547 15.217 15.277 125 15.307 VV 0.064 4771866 15.277 15.386 126 15.666 VV 0.044 3014914 15.600 15.673 127 15.684 VV 0.046 3678090 15.673 15.756 128 15.843 VV 0.051 6586107 15.777 15.869 129 15.876 VV 0.020 1476681 15.869 15.895 130 15.974 VV 0.063 53146600 15.895 16.096 131 16.156 VV 0.017 798780 16.145 16.175 132 16.274 VV 0.037 1890723 16.251 16.323 133 16.711 VV 0.059 3454193 16.670 16.756 134 16.774 VV 0.028 2412141 16.756 16.802 135 16.922 VV 0.029 2385467 16.882 16.934 136 17.296 VV 0.145 1204820912 16.934 17.339 137 17.350 VV 0.029 22254484 17.339 17.426 138 17.656 VV 0.019 1363377 17.635 17.665 139 17.694 VV 0.036 3738405 17.665 17.720 140 17.792 VV 0.046 13356010 17.720 17.812 141 17.937 VV 0.075 177086412 17.812 18.020 142 18.319 VV 0.036 2794738 18.260 18.325 143 18.351 VV 0.050 8465420 18.325 18.415 144 18.772 VV 0.080 156303979 18.575 18.832 145 18.883 VV 0.041 4864804 18.832 18.903 146 18.913 VV 0.017 1670150 18.903 18.924 147 18.979 VV 0.050 21302686 18.924 19.055 148 19.265 VV 0.057 3751800 19.202 19.308 149 19.457 VV 0.049 16120626 19.394 19.544 150 19.693 VV 0.024 985895 19.649 19.701 151 20.052 VV 0.035 1451265 20.024 20.084 152 20.096 VV 0.021 876168 20.084 20.120 153 20.624 PV 0.023 758052 20.598 20.660 154 22.038 PV 0.017 379541 22.022 22.051 155 22.514 VV 0.042 1130701 22.488 22.601 156 24.442 PV 0.018 695517 24.421 24.453 157 25.587 PV 0.022 616982 25.558 25.602